SEM image of a typical
AP-Grade sample. The strand-like fibers in this image are "ropes" of
parallel, individual single-walled carbon nanotubes (SWNT). Typical
rope diameter: ~20 nm. Typical SWNT diameter: ~1.4 nm. |
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| Single-Walled
Nanotube General Information
CarboLex AP-grade SWNT consists of single-walled, closed-ended, carbon nanotubes, which are made by Arc Method in specifically designed chambers. These carbon nanotubes are of average diameter 1.4nm and are found in “ropes” which are typically ~20nm in diameter or approximately 50 tubes per rope with lengths of 2 – 5 microns. Impurities include approximately 35w% residual catalyst (NI, Y) which is usually encapsulated in carbon shells. Some amorphous carbon may also be found on the outer surfaces of the ropes. The only post synthesis treatment of the nanotubes comes from the homogenization of the tubes directly from the chamber. Purity of CarboLex AP-grade SWNT is 50-70% and the purity of SE-grade SWNT is 70-90%. Chirality Information CarboLex AP-grade samples are mat (mixed) samples which include both semiconducting (-2/3) and metallic (-1/3) tubes with chiral angles distributed between 0 and 30. To determine the chiral angle, it is shown that electron diffraction measurements with suitable TEM instruments and using micro-diffraction techniques can provide detailed structural information on an individual single-walled nanotube. Another method to determine the tube chiral angle is atomic resolution STM. Summary of Thermal Conductivity of Nanotubes
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